SYNTHESIS AND SPECTROSCOPIC STUDIES OF AN AMINO ACID  BASED NLO  CRYSTAL:GLYCINE OXALATE

Dr Jyotsna Pandey

SYNTHESIS AND SPECTROSCOPIC STUDIES OF AN AMINO ACID BASED NLO CRYSTAL:GLYCINE OXALATE

June 2020

Vol-6, Issue-3

Paper ID: 12229

ISSN: 2395-4396

Downloads: 0

Abstract & Details

Research Area

science

Keywords

Glycine oxalic acid IR Raman 1H-NMR 13C-NMR

Abstract

A new organic NLO crystal GOA was synthesized by slow evaporation method. Glycine and oxalic acid were combined in different molar ratios to form glycine oxalic acid (GOA) transparent crystals of sizes (2-6 cm) in 2 to 3 weeks time. The solubility studies indicates a linear increase in solubility with increase in temperature from room temp to 75 0C. The phase formation using XRD studies shows orthorhombic crystal structure. The chemical contents of the crystals were verified by CHN analysis and are seen to agree with calculated chemical unit. The presence of two hydrogen atoms belonging to NH2 and CH2 group have been identified in 1H-NMR spectra and 13C-NMR Spectra confirms the presence of CH2 and COOH group .The IR &RAMAN assignments have been made for all the crystal and most of the peaks in IR are active in Raman indicating non-centro symmetric crystals.

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Author Information

#	Name	Institute / Affiliation
1	Dr Jyotsna Pandey	K C College,D W Road,Churchgate,Mumbai 20

How to Cite

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APA Style

Pandey, Dr Jyotsna (2020). SYNTHESIS AND SPECTROSCOPIC STUDIES OF AN AMINO ACID BASED NLO CRYSTAL:GLYCINE OXALATE. International Journal of Advance Research and Innovative Ideas In Education, 6(3), 1730-1738.

MLA Style

Pandey, Dr Jyotsna. "SYNTHESIS AND SPECTROSCOPIC STUDIES OF AN AMINO ACID BASED NLO CRYSTAL:GLYCINE OXALATE." International Journal of Advance Research and Innovative Ideas In Education, vol. 6, no. 3, 2020, pp. 1730-1738.

IEEE Style

Dr Jyotsna Pandey, "SYNTHESIS AND SPECTROSCOPIC STUDIES OF AN AMINO ACID BASED NLO CRYSTAL:GLYCINE OXALATE," International Journal of Advance Research and Innovative Ideas In Education, vol. 6, no. 3, pp. 1730-1738, 2020.

Vancouver Style

Pandey Dr Jyotsna. SYNTHESIS AND SPECTROSCOPIC STUDIES OF AN AMINO ACID BASED NLO CRYSTAL:GLYCINE OXALATE. International Journal of Advance Research and Innovative Ideas In Education. 2020;6(3):1730-1738.

Harvard Style

Pandey, Dr Jyotsna (2020) 'SYNTHESIS AND SPECTROSCOPIC STUDIES OF AN AMINO ACID BASED NLO CRYSTAL:GLYCINE OXALATE', International Journal of Advance Research and Innovative Ideas In Education, 6(3), pp. 1730-1738.

Chicago Style

Pandey, Dr Jyotsna. "SYNTHESIS AND SPECTROSCOPIC STUDIES OF AN AMINO ACID BASED NLO CRYSTAL:GLYCINE OXALATE." International Journal of Advance Research and Innovative Ideas In Education 6, no. 3 (2020): 1730-1738.

Turabian Style

Pandey, Dr Jyotsna. "SYNTHESIS AND SPECTROSCOPIC STUDIES OF AN AMINO ACID BASED NLO CRYSTAL:GLYCINE OXALATE." International Journal of Advance Research and Innovative Ideas In Education 6, no. 3 (2020): 1730-1738.